TY - JOUR T1 - Analytical characterization of recently excavated megalithic sarcophagi potsherds in Veeranam village, Tiruvannamalai dist., Tamilnadu, India JF - Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy Y1 - 2013 A1 - Ravisankar, R. A1 - Raja Annamalai, G. A1 - Naseerutheen, A. A1 - Chandrasekaran, A. A1 - Prasad, M.V.R. A1 - Satpathy, K.K. A1 - Maheswaran, C. KW - ED-XRF KW - Mineral Analysis KW - Pottery KW - SEM-EDX KW - Statistical Analysis KW - TG-DTA AB -

Analytical characterization of megalithic sarcophagi potsherds from Veeranam, Tiruvannamalai dist., Tamilnadu has been performed using Fourier transform infrared spectroscopy (FTIR), Powder X-ray diffraction (PXRD), Thermal analysis (TG-DTA), Scanning Electron Microscopy (SEM) coupled with an energy-dispersive X-ray spectrometer (EDX) and Energy dispersive X-ray fluorescence spectrometry (EDXRF). The EDXRF data of the potsherds were processed using multivariate statistical methods. Principal Component Analysis (PCA) and hierarchical cluster analysis allow us to identify grouping and structure in the data. The analytical results achieved in this study allowed us to estimate the firing temperature and manufacturing techniques. The methodological approach was successfully applied to the mineralogical, chemical and thermal characterization of the potsherds.

VL - 115 SP - 845 - 853 UR - http://www.sciencedirect.com/science/article/pii/S1386142513007373 J1 - Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy ID - AZ-CF-179505 M3 - 10.1016/j.saa.2013.06.123 SN - 13861425 ER -