The Abu Dhabi Authority for Culture and Heritage (ADACH) is responsible for the conservation and management of historic buildings and archaeological sites in the Emirate. Laboratory analysis has been critical for understanding the composition of historic materials and establishing appropriate conservation treatments across a wide variety of building types, ranging from Iron Age earthen archaeological sites to late-Islamic stone buildings. Analysis was carried out on historic sites in Al Ain, Delma Island and Liwa Oasis using techniques such as micro-x-ray fluorescence (MXRF), scanning electron microscopy/energy dispersive x-ray spectroscopy (SEM-EDX), polarized light microscopy (PLM), and x-ray diffraction (XRD). Testing was conducted through consultant laboratories and in collaboration with local universities. The initial aim of the analysis was to understand historic earthen materials and to confirm the suitability of locally sourced clays for the production of mud bricks and plasters. Another important goal was to characterize materials used in historic stone buildings in order to develop repair mortars, renders and grouts.